HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 18407322, compound → (4-Aminomethyl-2-methoxy-phenoxy)acetic Acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 18407322 | HCID 18407322 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | (4-Aminomethyl-2-methoxy-phenoxy)acetic Acid | HCID 13876411 | 55% |
Reaction Steps
A solution of 16 (0.276 g, 0.8 mmol) in MeOH (5 mL) was treated with 10% palladium on carbon (30 mg) and hydrogenated under a balloon of hydrogen for 30 min. The reaction mixture was filtrated and the filtrate was concentrated to give 17 as white solid (0.093 g, 55%) which was used to next step without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06476076B1 |
| Source dataset | uspto-grants-2002_11 |
| ORD ID | ord-ce7cf16934c843f7b86c9c2ad4b58d2e |
| Source note | uspto-grants-2002_11 |