HuagongsheHuagongshe Chemistry Print Report · For research reference only
Lithium Hydroxide → HCID 22038825, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Lithium Hydroxide | HCID 3939 | — |
| Reactant | HCID 86583530 | HCID 86583530 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 22038825 | HCID 22038825 | — |
Reaction Steps
The methyl (RS)-(4-carbamimidoyl-phenylamino)-(2-carbamoylmethoxy-5-ethoxy-phenyl)-acetate was saponified in THF with 1N LiOH to give (RS)-(4-carbamimidoyl-phenylamino)-(2-carbamoylmethoxy-5-ethoxy-phenyl)-acetic acid and purified by trituration in water and dilute ammonia; m.p. 266° C., MS: 387 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06476264B2 |
| Source dataset | uspto-grants-2002_11 |
| ORD ID | ord-95d8d845399442d4a3036190ced5d45e |
| Source note | uspto-grants-2002_11 |