N,N-Diethylethylenediamine → HCID 18001914, compound

HRID 1017296Notes

Reaction equation

HRID 1017296 reaction equation
[Cl:1][C:2]1[N:10]=[C:9]2[C:5]([N:6]=[CH:7][N:8]2[CH:11]2[CH2:15][CH2:14][CH2:13][CH2:12]2)=[C:4](Cl)[N:3]=1.[CH2:17]([N:19]([CH2:23][CH3:24])[CH2:20][CH2:21][NH2:22])[CH3:18]>C(N(CC)CC)C>[Cl:1][C:2]1[N:10]=[C:9]2[C:5]([N:6]=[CH:7][N:8]2[CH:11]2[CH2:15][CH2:14][CH2:13][CH2:12]2)=[C:4]([NH:22][CH2:21][CH2:20][N:19]([CH2:23][CH3:24])[CH2:17][CH3:18])[N:3]=1

Participants

4

Reactant 2

HCID 60993N,N-DiethylethylenediamineHCID 108011162,6-dichloro-9-cyclopentyl-9H-purine

Product 1

HCID 18001914HCID 18001914, compound

Reagents, catalysts & solvents 1

HCID 8471TriethylamineSolvent

Procedure

2-Chloro-6-[2-(diethylamino)ethylamino]-9-cyclopentylpurine is prepared from 2,6-dichloro-9-cyclopentylpurine, 2-diethylaminoethylamine, and triethylamine essentially as described above in Example 1, Scheme A, step b.

Sources & evidence

ORD record
ord-1c6e6fdaf39f4383baf67636fc39cf39
Source dataset
uspto-grants-2002_11
Patent number
US06479487B1

Reaction notes

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