Diglycolamine → HCID 54298436, compound

HRID 1017312Notes

Reaction equation

HRID 1017312 reaction equation
[Cl:1][C:2]1[N:10]=[C:9]2[C:5]([N:6]=[CH:7][N:8]2[CH:11]2[CH2:15][CH2:14][CH2:13][CH2:12]2)=[C:4](Cl)[N:3]=1.[NH2:17][CH2:18][CH2:19][O:20][CH2:21][CH2:22][OH:23]>C(N(CC)CC)C>[Cl:1][C:2]1[N:10]=[C:9]2[C:5]([N:6]=[CH:7][N:8]2[CH:11]2[CH2:15][CH2:14][CH2:13][CH2:12]2)=[C:4]([NH:17][CH2:18][CH2:19][O:20][CH2:21][CH2:22][OH:23])[N:3]=1

Participants

4

Reactant 2

HCID 13578DiglycolamineHCID 108011162,6-dichloro-9-cyclopentyl-9H-purine

Product 1

HCID 54298436HCID 54298436, compound

Reagents, catalysts & solvents 1

HCID 8471TriethylamineSolvent

Procedure

2-Chloro-6-(2-hydroxyethoxyethylamino)-9-cyclopentylpurine is prepared from 2,6-dichloro-9-cyclopentylpurine, 2-(2-aminoethoxy)ethanol, and triethylamine essentially as described above in Example 1, Scheme A, step b.

Sources & evidence

ORD record
ord-a3d4f2859d3347f2a6a6aad80613d65e
Source dataset
uspto-grants-2002_11
Patent number
US06479487B1

Reaction notes

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