Hydroxyamine hydrochloride → 1-(4-Propoxybutyl)-4-piperidone oxime

HRID 1017377Notes

Reaction equation

[CH2:1]([O:4][CH2:5][CH2:6][CH2:7][CH2:8][N:9]1[CH2:14][CH2:13][C:12](=O)[CH2:11][CH2:10]1)[CH2:2][CH3:3].Cl.[NH2:17][OH:18]>>[CH2:1]([O:4][CH2:5][CH2:6][CH2:7][CH2:8][N:9]1[CH2:14][CH2:13][C:12](=[N:17][OH:18])[CH2:11][CH2:10]1)[CH2:2][CH3:3]

Participants

Reactant 2

HCID 443297Hydroxyamine hydrochloride

HCID 180019641-(4-Propoxybutyl)-4-piperidone

Product 1

HCID 180019351-(4-Propoxybutyl)-4-piperidone oxime

Procedure

1-(4-Propoxybutyl)-4-piperidone oxime is prepared from 1-(4-propoxybutyl)-4-piperidone and hydroxylamine hydrochloride essentially as described above in Example 38, Scheme C, step b.

Sources & evidence

ORD record: ord-0f721941fb134136b5b4783ab0e02f49
Source dataset: uspto-grants-2002_11
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US06479487B1

Reaction notes

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