HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Methoxybenzaldehyde → 2-(4-Methoxyphenyl)quinazolin-4-ol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Methoxybenzaldehyde | HCID 31244 | — |
| Reactant | 2-(2-methoxyphenyl)-3H-quinazolin-4-one | HCID 135436005 | — |
| Product | 2-(4-Methoxyphenyl)quinazolin-4-ol | HCID 135430309 | 96.4% |
Reaction Steps
According to the preparation of 42, 4-methoxybenzaldehyde (35) (1.0 g, 7.3 mmol) was used to afford 44 (1.8 g, 96.4%) as pale yellow needles.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06479499B1 |
| Source dataset | uspto-grants-2002_11 |
| ORD ID | ord-aa4eb513259940a098c471432112a1e8 |
| Source note | uspto-grants-2002_11 |