HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetonitrile → HCID 9838264, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetonitrile | HCID 6342 | — |
| Reactant | Cyanoacetamide | HCID 7898 | — |
| Reactant | Ethyl Acetate | HCID 8857 | — |
| Reactant | Sodium Methoxide | HCID 10942334 | — |
| Reactant | HCID 12715559 | HCID 12715559 | — |
| Product | HCID 9838264 | HCID 9838264 | — |
Reaction Steps
In a similar manner to that of Example 26, 2-propoxyacetophenone (8.9 g) was allowed to react with ethyl acetate in the presence of sodium methoxide, and the intermediate was cyclised with cyanoacetamide to give the title compound, 0.2 g, m.p. 180°-180.5° C. (from acetonitrile).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06479520B1 |
| Source dataset | uspto-grants-2002_11 |
| ORD ID | ord-2e41650f2cd440d1897cf56cb6e7e905 |
| Source note | uspto-grants-2002_11 |