Dimethylformamide → HCID 18404783, compound

HRID 1017704Notes

Reaction equation

HRID 1017704 reaction equation
[CH2:1]([O:3][C:4]1[CH:9]=[CH:8][CH:7]=[CH:6][C:5]=1[C:10]1[NH:15][C:14](=[O:16])[C:13]([C:17]([NH2:19])=[O:18])=[CH:12][CH:11]=1)[CH3:2].[CH3:20]N(C)C=O>>[CH2:1]([O:3][C:4]1[CH:9]=[CH:8][CH:7]=[CH:6][C:5]=1[C:10]1[NH:15][C:14](=[O:16])[C:13]([C:17]([NH2:19])=[O:18])=[CH:12][CH:11]=1)[CH:2]=[CH2:20]

Participants

3

Reactant 2

HCID 6228DimethylformamideHCID 18404779HCID 18404779, compound

Product 1

HCID 18404783HCID 18404783, compound

Procedure

In a similar manner to that of Example 47, the product of Example 47 (1.89 g) gave the title compound, 1.74 g, m.p. 210°-212° C. (from dimethylformamide).

Sources & evidence

ORD record
ord-e69c56e0798b4b6a863d6ec6278a10d8
Source dataset
uspto-grants-2002_11
Patent number
US06479520B1

Reaction notes

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