HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 178420016, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Acetyl chloride | HCID 6367 | — |
| Reactant | Tert-butyl 4-(2H-tetrazol-5-YL)piperidine-1-carboxylate | HCID 18187701 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 178420016 | HCID 178420016 | — |
Reaction Steps
To 100 mg of the solid from Step A was added a solution of 0.30 mL of acetyl chloride in 5 mL of methanol (generates a methanol solution of hydrochloric acid). After 2.5 hours at room temperature, the reaction was evaporated to dryness, triturated twice with ether and vacuum dried to give the title compound as a tan solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06479518B2 |
| Source dataset | uspto-grants-2002_11 |
| ORD ID | ord-dc82687e5d16495b92ddfd81be3a0600 |
| Source note | uspto-grants-2002_11 |