HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 18404481, compound → HCID 18404459, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 18404481 | HCID 18404481 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 18404459 | HCID 18404459 | 41% |
Reaction Steps
The 197 mg of the product from Step A was taken up in 5 mL of methanol and hydrogenated at 40 psi over 60 mg of 10% Pd/C for 16 hours. The catalyst was removed by filtration and the solvent was removed in vacuo to afford 49 mg of title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06479518B2 |
| Source dataset | uspto-grants-2002_11 |
| ORD ID | ord-37197ac7437149aca72f8b3d3b6edaf2 |
| Source note | uspto-grants-2002_11 |