HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → HCID 18404976, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | HCID 18404979 | HCID 18404979 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Platinum | HCID 23939 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 18404976 | HCID 18404976 | — |
Reaction Steps
A suspension of 5.34 g (17.4 mmol) of N-(2-nitrophenyl)-4-bromo-2-methyl-aniline and 1.7 g of platinum on charcoal is stirred in 100 ml of dichloromethane and 100 ml of methanol at a hydrogen pressure of 3 bar for 1 hour. Then the catalyst is filtered off and the filtrate is evaporated down.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06479524B1 |
| Source dataset | uspto-grants-2002_11 |
| ORD ID | ord-0fbd836485324b7d8e7545ea167022f6 |
| Source note | uspto-grants-2002_11 |