Chloroform → HCID 18760473, compound

HRID 1017971Notes

Reaction equation

[CH2:1]([C:3]([NH2:12])([CH2:10][CH3:11])[CH2:4][NH:5][C:6]([CH3:9])([CH3:8])[CH3:7])[CH3:2].[CH2:13]([C:16]([CH2:18][CH2:19][CH3:20])=O)[CH2:14][CH3:15].[OH-:21].[Na+].[CH:23](Cl)(Cl)Cl>>[C:6]([N:5]1[CH2:4][C:3]([CH2:10][CH3:11])([CH2:1][CH3:2])[NH:12][C:16]([CH2:18][CH2:19][CH3:20])([CH2:13][CH2:14][CH3:15])[C:23]1=[O:21])([CH3:7])([CH3:9])[CH3:8]

Participants

Reactant 4

HCID 6212Chloroform

HCID 14798Sodium Hydroxide

HCID 312464-Heptanone

HCID 18760498HCID 18760498, compound

Product 1

HCID 18760473HCID 18760473, compound

Procedure

In analogy to Example B21, 1,1-diethyl-2-t-butylaminoethylamin, dipropylketon, chloroform and NaOH are reacted to give the title compound as a yellow oil.

Sources & evidence

ORD record: ord-4976a7d599784794a651711de4581390
Source dataset: uspto-grants-2002_11
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US06479608B1

Reaction notes

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