Imidazole → HCID 23322302, compound

HRID 1018418Notes

Reaction equation

HRID 1018418 reaction equation
[NH:1]1[CH:5]=[CH:4][N:3]=[CH:2]1.[NH:6]1[CH2:11][CH2:10][NH:9][CH2:8][CH2:7]1.[OH-].[Na+]>O>[NH:1]1[CH:5]=[CH:4][N:3]=[CH:2]1.[NH:6]1[CH2:11][CH2:10][NH:9][CH2:8][CH2:7]1

Participants

5

Reactant 3

HCID 795ImidazoleHCID 4837PiperazineHCID 14798Sodium Hydroxide

Product 1

HCID 23322302HCID 23322302, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

68.8 g (1.0 mole) of imidazole, 260.4 g (3.0 mole) of piperazine were solved in 699 ml of water and reacted with 370 g (4.0 mole) of epicholrhydrin as described in example no. 2 but at a pH of 7 which was held constant using NaOH.

Workup

  1. customreacted with 370 g (4.0 mole) of epicholrhydrin

Sources & evidence

ORD record
ord-afa70ccdd6244ef0a80bea912ba57a90
Source dataset
uspto-grants-2002_11
Patent number
US06482787B1

Reaction notes

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