HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Cyclohexen-1-one, 4,4-dimethyl- → Cyclohexanone, 4,4-dimethyl-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Cyclohexen-1-one, 4,4-dimethyl- | HCID 136839 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Pentane | HCID 8003 | — |
| Product | Cyclohexanone, 4,4-dimethyl- | HCID 138166 | — |
Reaction Steps
31.1 g of 4,4-dimethylcyclohex-2-enone in 100 ml of pentane are hydrogenated in an autoclave at a pressure of 5 bar in the presence of 1.6 g of 5% palladium on charcoal. The reaction mixture is filtered and the solvents are evaporated off under reduced pressure.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06482986B1 |
| Source dataset | uspto-grants-2002_11 |
| ORD ID | ord-881a17bc13424c8a8af2589d1eda0da5 |
| Source note | uspto-grants-2002_11 |