2-Cyclohexen-1-one, 4,4-dimethyl- → Cyclohexanone, 4,4-dimethyl-

HRID 1018794Notes

Reaction equation

HRID 1018794 reaction equation
[CH3:1][C:2]1([CH3:9])[CH2:7][CH2:6][C:5](=[O:8])[CH:4]=[CH:3]1>CCCCC.[Pd]>[CH3:1][C:2]1([CH3:9])[CH2:7][CH2:6][C:5](=[O:8])[CH2:4][CH2:3]1

Participants

4

Reactant 1

HCID 1368392-Cyclohexen-1-one, 4,4-dimethyl-

Product 1

HCID 138166Cyclohexanone, 4,4-dimethyl-

Reagents, catalysts & solvents 2

HCID 23938PalladiumCatalystHCID 8003PentaneSolvent

Procedure

31.1 g of 4,4-dimethylcyclohex-2-enone in 100 ml of pentane are hydrogenated in an autoclave at a pressure of 5 bar in the presence of 1.6 g of 5% palladium on charcoal. The reaction mixture is filtered and the solvents are evaporated off under reduced pressure.

Workup

  1. filtrationThe reaction mixture is filtered
  2. customthe solvents are evaporated off under reduced pressure

Sources & evidence

ORD record
ord-881a17bc13424c8a8af2589d1eda0da5
Source dataset
uspto-grants-2002_11
Patent number
US06482986B1

Reaction notes

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