O-Methylhydroxylamine → HCID 72591133, compound

Participants

Reaction Conditions

Reaction Steps

A solution of 21.7 g of the compound from Example 3 in 100 ml of methanol was admixed with 30.4 g of 30% strength aqueous methoxyamine solution and then stirred at 20-25° C. for 12 h. The solvent was distilled off and the residue was taken up in a mixture of methyl tert-butyl ether/water, and the phases were then separated. After drying, the solvent was removed from the organic phase. The residue gave 22 g of the title compound as a light-brown oil.

Provenance & Evidence