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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1018908Generated: October 30, 2026

Propylamine → HCID 15895895, compound

https://huagongshe.com/reaction/1018908

Reaction equation

Participants

RoleNameHCIDCharge
ReactantPropylamineHCID 7852—
ReactantHCID 88063986HCID 88063986—
SolventDiethyl EtherHCID 3283—
SolventAcetonitrileHCID 6342—
ProductHCID 15895895HCID 15895895—

Reaction Steps

A suspension of the compound obtained in Step E (1.26 g, 3.0 mmol) with n-propylamine (9.0 mmol) in 30 ml of acetonitrile is stirred for 3 hours. Evaporation to dryness is carried out, the residue is then taken up in 1N HCl and extraction is carried out with ethyl acetate. Drying over MgSO4 and evaporation of the organic phase yield a residue which is taken up in ether and filtered to yield the title product.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06486143B2
Source datasetuspto-grants-2002_11
ORD IDord-e2114d3d9a534ca1905f0fa4c6a6beef
Source noteuspto-grants-2002_11