HuagongsheHuagongshe Chemistry Print Report · For research reference only
Propylamine → HCID 15895895, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Propylamine | HCID 7852 | — |
| Reactant | HCID 88063986 | HCID 88063986 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 15895895 | HCID 15895895 | — |
Reaction Steps
A suspension of the compound obtained in Step E (1.26 g, 3.0 mmol) with n-propylamine (9.0 mmol) in 30 ml of acetonitrile is stirred for 3 hours. Evaporation to dryness is carried out, the residue is then taken up in 1N HCl and extraction is carried out with ethyl acetate. Drying over MgSO4 and evaporation of the organic phase yield a residue which is taken up in ether and filtered to yield the title product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06486143B2 |
| Source dataset | uspto-grants-2002_11 |
| ORD ID | ord-e2114d3d9a534ca1905f0fa4c6a6beef |
| Source note | uspto-grants-2002_11 |