Benzoyl Peroxide → HCID 18398678, compound

Participants

Reaction Steps

To the compound of Step 2 (0.122 g, 0.400 mmol) in CCl4 (5 mL) were added NBS (0.050 g, 0.480 mle) and a catalytic amount of benzoyl peroxide. The reaction mixture was refluxed under light for 2 h. The reaction was cooled to room temperature, filtered and evaporated. The title compound was obtained after purification by flash chromatography. (0.150 g).

Provenance & Evidence