HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium → (Z)-3-methoxy4-acetoxystyryl-2,4,5-trimethoxybenzylsulfide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium | HCID 5360545 | — |
| Reactant | (2,4,5-Trimethoxyphenyl)methanethiol | HCID 10488827 | — |
| Reactant | 3-Methoxy-4-acetoxyphenylacetylene | HCID 22603806 | — |
| Product | (Z)-3-methoxy4-acetoxystyryl-2,4,5-trimethoxybenzylsulfide | HCID 86585665 | — |
Reaction Steps
A solution of 3-methoxy-4-acetoxyphenylacetylene (0.02 mol), 2,4,5-trimethoxybenzyl mercaptan (0.02 mol) and metallic sodium (0.02 g atom) is subjected to General Procedure 2 to form (Z)-3-methoxy-4-acetoxystyryl-2,4,5-trimethoxybenzylsulfide. The title compound is obtained following oxidation of the sulfide, according to General Procedure 2.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06486210B2 |
| Source dataset | uspto-grants-2002_11 |
| ORD ID | ord-7ecf269cd7b049f6ae3063e401fa8a19 |
| Source note | uspto-grants-2002_11 |