HuagongsheHuagongshe Chemistry Print Report · For research reference only
m-Chloroperbenzoic acid → HCID 131723658, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | m-Chloroperbenzoic acid | HCID 70297 | — |
| Reactant | HCID 131723659 | HCID 131723659 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 131723658 | HCID 131723658 | — |
Reaction Steps
A mixture of 1.68 g (6.83 mmol) of compound obtained from step A, 1.24 g (7.17 mmol) of m-chloroperbenzoic acid was dissolved in 100 mL of methylene chloride and stirred at room temperature for 4 hours. After 4 filtration, the filtrate was washed with 10 mL of 1 N NaOH solution, brine, dried and evaporated to give title product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06486201B1 |
| Source dataset | uspto-grants-2002_11 |
| ORD ID | ord-352c4ec2dda9475599fd21309aaceb8a |
| Source note | uspto-grants-2002_11 |