Aluminium lithium hydride → HCID 15513019, compound

Participants

Reaction Steps

To a suspension of 0.69 g (18.3 mmol) of LiAlH4 in 150 mL of anhydrous ether cooled with ice bath was added a solution of the compound obtained from step B in anhydrous ether. The reaction mixture was stirred for 30 min. with cooling, 3 hours at room temperature, then quenched with water saturated ether and 2 mL of 10% NaOH solution. After filtration, the solvent was removed by evaporation to give title product.

Provenance & Evidence