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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1019350Generated: October 31, 2026

4-Iodophenol → HCID 18401150, compound

https://huagongshe.com/reaction/1019350

Reaction equation

Participants

RoleNameHCIDCharge
Reactant4-IodophenolHCID 10894—
ReactantPotassium CarbonateHCID 11430—
ReactantN-3-BromopropylphthalimideHCID 21611—
SolventAcetonitrileHCID 6342—
ProductHCID 18401150HCID 18401150—

Reaction Steps

N-(3-bromopropyl)phthalimide (1 eq., Aldrich), 4-iodophenol (1 eq., Aldrich) and potassium carbonate (2 eq.) were stirred in acetonitrile. The mixture was heated at reflux. After 64 hours, the reaction mixture was concentrated to a thick mixture which was slurried in water. A white solid was collected, washed with water and vacuum dried to provide 1-(4-iodophenoxy)-3-(phthalimido)propane.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06486350B1
Source datasetuspto-grants-2002_11
ORD IDord-9a1570c1ed554772b415e454b13488a7
Source noteuspto-grants-2002_11