HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Iodophenol → HCID 18401150, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Iodophenol | HCID 10894 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | N-3-Bromopropylphthalimide | HCID 21611 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 18401150 | HCID 18401150 | — |
Reaction Steps
N-(3-bromopropyl)phthalimide (1 eq., Aldrich), 4-iodophenol (1 eq., Aldrich) and potassium carbonate (2 eq.) were stirred in acetonitrile. The mixture was heated at reflux. After 64 hours, the reaction mixture was concentrated to a thick mixture which was slurried in water. A white solid was collected, washed with water and vacuum dried to provide 1-(4-iodophenoxy)-3-(phthalimido)propane.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06486350B1 |
| Source dataset | uspto-grants-2002_11 |
| ORD ID | ord-9a1570c1ed554772b415e454b13488a7 |
| Source note | uspto-grants-2002_11 |