Pyrazole → HCID 178506974, compound

HRID 1019464Notes

Reaction equation

HRID 1019464 reaction equation
[NH:1]1[CH:5]=[CH:4][CH:3]=[N:2]1.[Li:6][S:7]([O:10][C:11]([F:14])([F:13])[F:12])(=[O:9])=[O:8]>>[NH:1]1[CH:5]=[CH:4][CH:3]=[N:2]1.[Li:6][S:7]([O:10][C:11]([F:14])([F:13])[F:12])(=[O:9])=[O:8]

Participants

3

Reactant 2

HCID 1048PyrazoleHCID 178506973HCID 178506973, compound

Product 1

HCID 178506974HCID 178506974, compoundYield 160.1%

Conditions

Temperature
50 °C

Procedure

2.61 g of purified pyrazole and 2 g of LiSO3CF3 were put into a round bottom flask and slowly stirred for 50 minutes under a nitrogen circumstance of 50° C., thereby obtaining 4.6 g of pyrazole-LiSO3CF3 eutectic mixture.

Sources & evidence

ORD record
ord-4d829da5503a4196b0f3ccab996f08bb
Source dataset
uspto-grants-2014_05
Patent number
US08715866B2

Reaction notes

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