Hydrochloric Acid → HCID 67481568, compound

Participants

Reaction Steps

To 2.2 (0.05 g, 0.099 mmol) in dioxane (0.331 mL) was added lithium hydroxide monohydrate (6.25 mg, 0.149 mmol) in water (0.331 mL). The reaction was stirred at room temperature for 1 hour. The reaction was then acidified with 1N HCl and diluted with DCM. The organic layer was extracted, dried over Na2SO4, filtered and concentrated to provide 2.3 as a light yellow solid. ESI-MS M+H 490.0.

Provenance & Evidence