HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 66661106, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 66660979 | HCID 66660979 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 66661106 | HCID 66661106 | — |
Reaction Steps
The process is performed according to the procedure described in Example 11 (step 11.2.). Starting with 1.30 g (3.40 mmol) of tert-butyl 3-[(3-methylcarbamoylisoxazol-5-ylmethoxycarbonylamino)methyl]pyrrolidine-1-carboxylate and 4.25 mL of hydrogen chloride as a 4N solution in dioxane, and after triturating in diethyl ether, 0.82 g of a white powder is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08716289B2 |
| Source dataset | uspto-grants-2014_05 |
| ORD ID | ord-094181da029641039d4516f13cb623f3 |
| Source note | uspto-grants-2014_05 |