Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 3-Pentanamine | HCID 12019 | — |
| Reactant | 3-Chloroquinoxalin-2-amine | HCID 817274 | — |
| Product | HCID 57880837 | HCID 57880837 | 78% |
Reaction Steps
A thick-walled microwave bottle equipped with a stirbar was charged with 3-chloroquinoxalin-2-amine (1.0 equiv) and 20 volume equivalents of 3-aminopentane. The bottle was fitted with a septum and cap and heated to 120° C. in a microwave for 30 min. The resulting solution was concentrated in vacuo. Flash chromatography (20%-60% EtOAc/Hexanes) provided the title compound (78%) as a yellow solid. LCMS m/z (APCI)=231.1 (M+H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US08716291B2 |
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| Source dataset | uspto-grants-2014_05 |
|---|
| ORD ID | ord-1e61282e350a48feaf37d6470e9eb49d |
|---|
| Source note | uspto-grants-2014_05 |
|---|
