HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 67467810, compound → HCID 67468959, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 67467810 | HCID 67467810 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 67468959 | HCID 67468959 | — |
Reaction Steps
Benzyl-[2-(4-nitro-phenyl)-ethyl]-carbamic acid tert-butyl ester (100 mmol) was dissolved in THF (20 ml) and hydrogenated under a pressure of one atmosphere overnight. The reaction mixture was filtered and washed with THF. The filtrate was concentrated to dryness and was used directly in the procedure for Example 1D.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08716287B2 |
| Source dataset | uspto-grants-2014_05 |
| ORD ID | ord-6dff9948bda044958b3526fbc702b2be |
| Source note | uspto-grants-2014_05 |