HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thiourea → HCID 131731372, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thiourea | HCID 2723790 | — |
| Reactant | HCID 21111669 | HCID 21111669 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 131731372 | HCID 131731372 | 95% |
Reaction Steps
4-Bromobutyl pivalate (0.71 mol) and thiourea (0.78 mol) were dissolved in ethanol (330 ml) and the resulting mixture was refluxed for 1 h. The solvent was removed under vacuum. The resulting residue was used in the next step without further purification. Yield: 210 g (95% yield).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08716293B2 |
| Source dataset | uspto-grants-2014_05 |
| ORD ID | ord-c3fa1d267e3c49918c0604b06e3de9a5 |
| Source note | uspto-grants-2014_05 |