Hydrochloric Acid → HCID 66599998, compound

HRID 1020135Notes

Reaction equation

HRID 1020135 reaction equation
C1(C(=[N:14][CH2:15][C:16]([CH3:27])([C:21]2[CH:26]=[CH:25][CH:24]=[CH:23][CH:22]=2)[C:17]([O:19]C)=[O:18])C2C=CC=CC=2)C=CC=CC=1.[ClH:28]>>[ClH:28].[NH2:14][CH2:15][C:16]([CH3:27])([C:21]1[CH:26]=[CH:25][CH:24]=[CH:23][CH:22]=1)[C:17]([OH:19])=[O:18]

Participants

3

Procedure

A mixture of methyl 3-(diphenylmethyleneamino)-2-methyl-2-phenylpropanoate (E321) and 6 N HCl was refluxed overnight. The solution was cooled and evaporated to give 3-amino-2-methyl-2-phenylpropanoic acid hydrochloride (E322).

Workup

  1. temperaturewas refluxed overnight
  2. temperatureThe solution was cooled
  3. customevaporated

Sources & evidence

ORD record
ord-0b96a2fb2acf41f2bb21eee6f47f26ed
Source dataset
uspto-grants-2014_05
Patent number
US08716310B2

Reaction notes

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