Methylparaben → HCID 57461804, compound

HRID 1020361Notes

Reaction equation

Cl[C:2]1[CH:7]=[CH:6][C:5]([N+:8]([O-])=O)=[CH:4][N:3]=1.[OH:11][C:12]1[CH:21]=[CH:20][C:15]([C:16]([O:18][CH3:19])=[O:17])=[CH:14][CH:13]=1>>[NH2:8][C:5]1[CH:6]=[CH:7][C:2]([O:11][C:12]2[CH:13]=[CH:14][C:15]([C:16]([O:18][CH3:19])=[O:17])=[CH:20][CH:21]=2)=[N:3][CH:4]=1

Participants

Reactant 2

HCID 7456Methylparaben

HCID 783082-Chloro-5-nitropyridine

Product 1

HCID 57461804HCID 57461804, compound

Procedure

Intermediate B-32 was prepared by the general procedure for intermediate B-2, by using 2-chloro-5-nitropyridine and methyl 4-hydroxybenzoate as starting materials. MS (M+1): 245.

Workup

customIntermediate B-32 was prepared by the general procedure for intermediate B-2

Sources & evidence

ORD record: ord-25106ce8423d48c5a750311e3ceb491d
Source dataset: uspto-grants-2014_05
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US08716312B2

Reaction notes

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