HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Chloro-5-nitropyridine → tert-Butyl 1-(5-aminopyridin-2-yl)piperidin-4-ylcarbamate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Chloro-5-nitropyridine | HCID 78308 | — |
| Reactant | 4-(N-Boc-amino)piperidine | HCID 723833 | — |
| Product | tert-Butyl 1-(5-aminopyridin-2-yl)piperidin-4-ylcarbamate | HCID 22557725 | — |
Reaction Steps
Intermediate B-33 was prepared by the general procedure for intermediate B-2, by using 2-chloro-5-nitropyridine and tert-butyl piperidin-4-ylcarbamate as the starting material. LCMS [M+1]+ 293.2.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08716312B2 |
| Source dataset | uspto-grants-2014_05 |
| ORD ID | ord-c32786c8c6a84a5c9c14f4c6f8483dcb |
| Source note | uspto-grants-2014_05 |