Cyclopentanemethanol → HCID 67391968, compound

Participants

Reaction Steps

Compound 287 was prepared by the general procedure for compound 284, by using intermediates A-41 and cyclopentanemethanol as starting materials. 1H NMR (500 MHz, CDCl3) δ 8.20 (d, 1H, J=2.4 Hz), 8.07 (dd, 1H, J=9.2, 2.5 Hz), 7.23 (br s, 1H), 6.68 (d, 1H, J=9.1 Hz), 5.17 (m, 1H), 4.45 (d, 2H, J=9.1 Hz), 3.64-3.52 (m, 8H), 2.45 (m, 1H), 1.92-1.84 (m, 4H), 1.80-1.56 (m, 10H), 1.42-1.32 (m, 2H); LCMS (ESI) Rt=4.13 min, calcd for [M+1]+ 552.2. found 552.3.

Provenance & Evidence