Hydroxyamine hydrochloride → HCID 49805675, compound

Participants

Reaction Steps

The procedure of the step 3 in Example 80 was repeated except that 6-(2-methyl-3-(2,4-dimethoxyphenyl)-benzamido)hexanoic acid instead of 6-(3-bromo-2-methylbenzamido)hexanoic acid, and hydroxylamine hydrochloride instead of 1,2-phenylenediamine were used and purified by a preparative HPLC (C18, 20% H2O/CH3CN, 20 ml/min) to obtain the title compound (27 mg, 35%).

Provenance & Evidence