Hydrochloric Acid → HCID 68656833, compound

Participants

Reaction Steps

2 N HCl in Et2O (0.12 mL, 0.24 mmol) was added to a solution of 4-(4-methoxyphenyl)-1-(5-methyl-2,3,4,5-tetrahydro-1H-pyrido[4,3-b]indol-7-yl)pyridin-2(1H)-one (45 mg, 0.12 mmol) in CH2Cl2 (2.0 mL), and the solution was stirred at ambient temperature for 2.5 h under N2. The reaction mixture was concentrated, partially diluted with H2O and lyophilized to provide the title compound (46 mg, 95%) as a yellow powder:

Provenance & Evidence