Hydrochloric Acid → HCID 66797470, compound

Participants

Reaction Steps

To an ice cold solution of 4-[2-(Benzyl-methyl-amino)-quinoxalin-6-yl]-pyrazole-1-carboxylic acid tert-butyl ester (250 mg) in 1,4-dioxane (3 mL), HCl (in 1,4-dioxane) was added. The resulting mixture was allowed to warm to RT and was stirred further for 2 hours. After completion of the reaction the volatiles were evaporated under vacuum and the HCl salt of the final compound was triturated with DCM. The product was further purified by preparative HPLC (0.009 g, 3%).

Provenance & Evidence