HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 58946436, compound → HCID 57686422, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 58946436 | HCID 58946436 | — |
| Solvent | Trifluoroacetic acid methylene chloride | HCID 21863450 | — |
| Product | HCID 57686422 | HCID 57686422 | 217.2% |
Reaction Steps
3-Methylsulfanyl-pyrrolidine-1,3-dicarboxylic acid 1-tert-butyl ester 3-methyl ester (2.15 gm, 8.8 mmol) was dissolved in 20 ml of 50% trifluoroacetic acid/dichloromethane and stirred for 2 hrs. The reaction mixture was evaporated to give 3.35 g of 3-Methylsulfanyl-pyrrolidine-3-carboxylic acid methyl ester 4BP as a gummy solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08716483B2 |
| Source dataset | uspto-grants-2014_05 |
| ORD ID | ord-8558cd3469b44ba6a94ed26880965610 |
| Source note | uspto-grants-2014_05 |