HuagongsheHuagongshe Chemistry Print Report · For research reference only
trans-Stilbene → Stilbene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | trans-Stilbene | HCID 638088 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | Stilbene | HCID 11502 | — |
Reaction Steps
Into a 30 mL two-neck flask, a methanol solution (0.04 g/L, 70 μL) of the [HPS-N(C2H4OC2H4OCH3)3Br]Pt particle complex prepared in Example 17 and 180 mg of trans-stilbene were charged and thereto, 2 mL of methanol was added. The inside of the system was purged with hydrogen and the reaction was effected at room temperature for 11 hours. A dibenzyl derived from reduction of trans-stilbene was obtained in a yield measured by G.C. of 93%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08722562B2 |
| Source dataset | uspto-grants-2014_05 |
| ORD ID | ord-9d925e81eb1d401ca6042cdccf707c34 |
| Source note | uspto-grants-2014_05 |