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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1022657Generated: October 30, 2026

Methyl chloroacetate → HCID 85706506, compound

https://huagongshe.com/reaction/1022657

Reaction equation

Participants

RoleNameHCIDCharge
ReactantMethyl chloroacetateHCID 7295—
Reactant3,4-DichlorobenzaldehydeHCID 22710—
ReactantSodium methanolate methanolHCID 23694274—
SolventMethanolHCID 887—
ProductHCID 85706506HCID 85706506—

Reaction Steps

To a solution of 3,4-dichlorobenzaldehyde (51.0 g) and methyl chloroacetate (51 mL) in methanol (500 mL) was added 28% sodium methoxide/methanol (68 mL) solution under ice-cooling, and the mixture was stirred at room temperature overnight. The resultant product was collected by filtration, and washed with distilled water to give the title compound (90.9 g).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08722662B2
Source datasetuspto-grants-2014_05
ORD IDord-320308a3e3694e529aef9ab12a06f3f3
Source noteuspto-grants-2014_05