HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl chloroacetate → HCID 85706506, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl chloroacetate | HCID 7295 | — |
| Reactant | 3,4-Dichlorobenzaldehyde | HCID 22710 | — |
| Reactant | Sodium methanolate methanol | HCID 23694274 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 85706506 | HCID 85706506 | — |
Reaction Steps
To a solution of 3,4-dichlorobenzaldehyde (51.0 g) and methyl chloroacetate (51 mL) in methanol (500 mL) was added 28% sodium methoxide/methanol (68 mL) solution under ice-cooling, and the mixture was stirred at room temperature overnight. The resultant product was collected by filtration, and washed with distilled water to give the title compound (90.9 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08722662B2 |
| Source dataset | uspto-grants-2014_05 |
| ORD ID | ord-320308a3e3694e529aef9ab12a06f3f3 |
| Source note | uspto-grants-2014_05 |