HRID1022726

反应详情

EQUATION

反应方程式

HRID 1022726 的结构方程式

PROCEDURE

实验过程

To tert-butyl (6R,7S)-6-(benzylamino)-7-(3,4-dichlorophenyl)-1,4-oxazepane-4-carboxylate (80 mg) was added 4.0 M hydrogen chloride-ethyl acetate solution (4 mL), and the mixture was stirred at room temperature for 1 hr. The residue obtained by concentration under reduced pressure was washed with diethyl ether to give the title compound (20 mg).

WORKUP

后处理

  1. customThe residue obtained by concentration under reduced pressure
  2. washwas washed with diethyl ether