HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethyl N-cyanodithioiminocarbonate → HCID 178503898, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethyl N-cyanodithioiminocarbonate | HCID 66289 | — |
| Reactant | Benzo-1,3-dioxole-5-methylamine | HCID 75799 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 178503898 | HCID 178503898 | 95% |
Reaction Steps
1.6 g (10.94 mmol) of dimethyl cyanocarbonodithioimidate and 2.0 g (13.23 mmol) of piperonyl amine were dissolved in methyl alcohol, and then stirred for 30 minutes. After completion of the reaction, the produced solid was filtered, and then washed with water and methyl alcohol, thus obtaining 2.4 g (95% yield) of a desired compound of Formula 3.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08722674B2 |
| Source dataset | uspto-grants-2014_05 |
| ORD ID | ord-e03ebf047c90496abd7dd657bccab0f9 |
| Source note | uspto-grants-2014_05 |