HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,4-Benzodioxane-6-carboxylic Acid → HCID 178523674, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,4-Benzodioxane-6-carboxylic Acid | HCID 2758833 | — |
| Reactant | HCID 178478587 | HCID 178478587 | — |
| Product | HCID 178523674 | HCID 178523674 | — |
Reaction Steps
The title compound, white solid (19 mg, 47.2%), MS (ISP) m/z=494.3 [(M+H)+], was prepared in accordance with the general method of example 1 from Trans-4-[2-(4-Benzo[1,3]dioxol-4-yl-piperazin-1-yl)-ethyl]-cyclohexylamine hydrochloride (Intermediate A) (30 mg, 81.5 mmol) and 2,3-dihydrobenzo[b][1,4]dioxine-6-carboxylic acid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08722683B2 |
| Source dataset | uspto-grants-2014_05 |
| ORD ID | ord-33d1b90b8c414001bc37fc70e32f9588 |
| Source note | uspto-grants-2014_05 |