HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-methyl-1H-imidazole-4-sulfonyl chloride → HCID 178481302, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-methyl-1H-imidazole-4-sulfonyl chloride | HCID 2736887 | — |
| Reactant | HCID 178478587 | HCID 178478587 | — |
| Product | HCID 178481302 | HCID 178481302 | — |
Reaction Steps
The title compound, white solid (23 mg, 59.3%), MS (ISP) m/z=476.1 [(M+H)+], was prepared in accordance with the general method of example 66 from N-trans-4-[2-(4-Benzo[1,3]dioxol-4-yl-piperazin-1-yl)-ethyl]-cyclohexylamine hydrochloride (Intermediate A) (30 mg, 81.5 μmol) and 1-methyl-1H-imidazole-4-sulfonyl chloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08722683B2 |
| Source dataset | uspto-grants-2014_05 |
| ORD ID | ord-74529c8d9da044dd8e8ac4d77618c7f7 |
| Source note | uspto-grants-2014_05 |