HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl(4-aminophenoxy)acetate → Methyl 4-[(4,5-diisopropylfuran-2-carbonyl)amino]phenyloxyacetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl(4-aminophenoxy)acetate | HCID 6422115 | — |
| Reactant | 4,5-Diisopropylfuran-2-carboxylic acid | HCID 58420514 | — |
| Product | Methyl 4-[(4,5-diisopropylfuran-2-carbonyl)amino]phenyloxyacetate | HCID 67396770 | 86% |
Reaction Steps
In the same manner as that of Example 2, 4,5-diisopropylfuran-2-carboxylic acid (60 mg, 0.306 mmol) was condensed with methyl 4-aminophenoxyacetate, and the resultant was purified by silica gel chromatography (0.5% methanol-chloroform) to obtain methyl 4-[(4,5-diisopropylfuran-2-carbonyl)amino]phenyloxyacetate (94 mg, 86%) as colorless needles.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08722730B2 |
| Source dataset | uspto-grants-2014_05 |
| ORD ID | ord-defa4d11189149e19ca48c60bfedc7e5 |
| Source note | uspto-grants-2014_05 |