HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl 4-aminobenzoate → HCID 67394987, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl 4-aminobenzoate | HCID 12082 | — |
| Reactant | HCID 58420519 | HCID 58420519 | — |
| Product | HCID 67394987 | HCID 67394987 | 86.3% |
Reaction Steps
In the same manner as that of Example 2, 4,5-diisopropylthiophene-2-carboxylic acid (86 mg, 0.406 mmol) was condensed with methyl 4-aminobenzoate (123 mg, 0.815 mmol), and the resultant was purified by silica gel chromatography [hexane-ethyl acetate (3:1)] to obtain methyl 4-[(4,5-diisopropylthiophene-2-carbonyl)amino]benzoate (121 mg, 86%) as colorless needles.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08722730B2 |
| Source dataset | uspto-grants-2014_05 |
| ORD ID | ord-7e56b4e3042b4db4b0b42d7b7e29cf44 |
| Source note | uspto-grants-2014_05 |