HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 25189596, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 67395328 | HCID 67395328 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 25189596 | HCID 25189596 | 87.2% |
Reaction Steps
A solution of the aforementioned ester (92 mg, 0.265 mmol) in ethanol (5 ml) was added with 2 M aqueous sodium hydroxide (1 ml) to perform hydrolysis at room temperature for 4 hours, and extraction and recrystallization were performed to obtain the title compound (22, 77 mg, 86%) as colorless needles.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08722730B2 |
| Source dataset | uspto-grants-2014_05 |
| ORD ID | ord-b7bab5cf577f4413bcda15187f6484c1 |
| Source note | uspto-grants-2014_05 |