HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → HCID 59191207, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | Propylamine | HCID 7852 | — |
| Reactant | HCID 59191297 | HCID 59191297 | — |
| Product | HCID 59191207 | HCID 59191207 | 41% |
Reaction Steps
According to the procedure of example 65(b) except substituting 4-(4-ethyl-2-methoxyphenoxy)-3-fluorobenzene sulfonyl chloride for 4-[2-(benzyloxy)-4-ethylphenoxy]-3-fluorobenzene sulfonyl chloride and NH3 for propylamine (1.7 mmol; 0.14 mL), the title compound (140 mg; 0.32 mmol; 41%) was obtained as a brown oil after purification on preparative TLC (dichloromethane).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08722746B2 |
| Source dataset | uspto-grants-2014_05 |
| ORD ID | ord-7b1c162527e3499095ac13e9d2e1894b |
| Source note | uspto-grants-2014_05 |