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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1023967Generated: October 29, 2026

Tetrahydrofuran → HCID 59191412, compound

https://huagongshe.com/reaction/1023967

Reaction equation

Participants

RoleNameHCIDCharge
ReactantTetrahydrofuranHCID 8028—
ReactantHCID 59191207HCID 59191207—
SolventEthanolHCID 702—
ProductHCID 59191412HCID 5919141262%

Reaction Steps

According to the procedure of example 20(b) except substituting 4-ethyl-2-methoxy-1-[4-nitro-2-(trifluoromethyl)phenoxy]benzene for 4-(2-Benzyloxy-4-ethyl-phenoxy)-3-fluoro-N-propyl-benzenesulfonamide (140 mg; 0.32 mmol) and tetrahydrofurane for ethanol (3 mL), the title compound (70 mg; 62%) was obtained as a clear oil, after purification on preparative TLC (dichloromethane)

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08722746B2
Source datasetuspto-grants-2014_05
ORD IDord-425c40518f484db0a4936c8d74828b65
Source noteuspto-grants-2014_05