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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1023988Generated: October 30, 2026

Tetrahydrofuran → HCID 59191341, compound

https://huagongshe.com/reaction/1023988

Reaction equation

Participants

RoleNameHCIDCharge
ReactantTetrahydrofuranHCID 8028—
ReactantHCID 59191301HCID 59191301—
SolventEthanolHCID 702—
ProductHCID 59191341HCID 59191341—

Reaction Steps

According to the procedure of example 20(b) except substituting 4-ethyl-2-methoxy-1-[4-nitro-2-(trifluoromethyl)phenoxy]benzene by 2-{[4-(2-fluoro-4-nitrophenoxy)-3-methoxy phenyl]ethynyl}pyridine (0.23 mmol; 84 mg) and THF by ethanol, the title compound was obtained as a clear oil (68%, 53 mg) 10 after purification on preparative TLC (cyclohexane/ethyl acetate: 6/4).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08722746B2
Source datasetuspto-grants-2014_05
ORD IDord-726aafa15db848c480ecdc7cdf61f812
Source noteuspto-grants-2014_05