Water → HCID 87329530, compound

Participants

Reaction Steps

H(CF2)6CH2SO2H (1.00 g, 2.63 mmol) was put in a 100 ml flask, and was dissolved in acetic acid (20 ml) in the air. After the reaction system was dipped in ice bath and water (1.0 ml) was added thereto, bromine (1.1 g, 6.84 mmol) was added and stirring was continued at room temperature for 12 hours. After completion of the reaction, the inside of the system was brought to reduced pressure, and after removing the solvent and bromine, the reaction product was dried in vacuo at 60° C. for 12 hours to obtain H(CF2)6CH2SO3H (1.04 g, 2.63 mmol).

Provenance & Evidence