Indene → HCID 6713780, compound

HRID 1024127Notes

Reaction equation

HRID 1024127 reaction equation
[CH3:1][C:2]([C:4]1[CH:9]=[CH:8][CH:7]=[CH:6][CH:5]=1)=[CH2:3].[CH2:10]1[C:18]2[C:13](=[CH:14][CH:15]=[CH:16][CH:17]=2)[CH:12]=[CH:11]1>>[CH3:3][C:2]([C:4]1[CH:9]=[CH:8][CH:7]=[CH:6][CH:5]=1)=[CH2:1].[CH2:10]1[C:18]2[C:13](=[CH:14][CH:15]=[CH:16][CH:17]=2)[CH:12]=[CH:11]1

Participants

3

Reactant 2

HCID 7219Indene2×HCID 7407Alpha-Methylstyrene2×

Product 1

HCID 6713780HCID 6713780, compound

Conditions

Temperature
12.5 °C

Procedure

A resin M-1 is prepared in a manner similar to that of preparing the resin I-1, except that 54 g of α-methylstyrene and 36 g of indene (that is, α-methylstyrene: 60 mass %, indene: 40 mass %) are used and that the addition of the catalyst is carried for 15 minutes and the polymerization reaction is allowed to proceed for 1 hour in a state where the temperature of the reaction mixed solution is maintained in the range of 10 to 15° C. The α-methylstyrene/indene copolymer resin thus obtained has yield: 86 g, softening point: 165° C., number-average molecular weight (Mn): 1000, and weight-average molecular weight (Mw): 3000.

Workup

  1. customA resin M-1 is prepared in a manner similar to that
  2. customof preparing the resin I-1
  3. customthe polymerization reaction
  4. waitto proceed for 1 hour in a state where
  5. additionthe temperature of the reaction mixed solution

Sources & evidence

ORD record
ord-673ac7b9921a40f8a1fa333a5b560c73
Source dataset
uspto-grants-2014_05
Patent number
US08722806B2

Reaction notes

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